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Preparation and characterization of novel carbon molecular sieve membrane/PSSF composite by pyrolysis method for toluene adsorption

Ying Yan, Peng Huang, Huiping Zhang

《化学科学与工程前沿（英文）》 2019年 第13卷 第4期   页码 772-783 doi: 10.1007/s11705-019-1827-y

摘要： Carbon molecular sieve membrane (CMSM)/paper-like stainless steel fibers (PSSF) has been manufactured by pyrolyzing poly (furfuryl alcohol) (PFA) coated on the metal fibers. PFA was synthesized using oxalic acid dihydrate as a catalyst and coated on microfibers by dip coating method. For the purpose of investigating the effects of final carbonization temperature, the composites were carbonized between 400°C and 800°C under flowing nitrogen. The morphology and microstructure were examined by X-ray diffraction, Fourier transforms infrared spectroscopy, scanning electron microscopy, thermogravimetric analysis, N adsorption and desorption, Raman spectra and X-ray photoelectron spectra. The consequences of characterization showed that the CMSM containing mesopores of 3.9 nm were manufactured. The specific surface area of the CMSM/PSSF fabricated in different pyrolysis temperature varies from 26.5 to 169.1 m ∙g and pore volume varies from 0.06 to 0.23 cm ∙g . When pyrolysis temperature exceeds 600°C, the specific surface, pore diameter and pore volume decreased as carbonization temperature increased. Besides, the degree of graphitization in carbon matrix increased with rising pyrolysis temperature. Toluene adsorption experiments on different structured fixed bed that was padded by CMSM/PSSF and granular activated carbon (GAC) were conducted. For the sake of comparison, adsorption test was also performed on fixed bed packed with GAC. The experimental results indicated that the rate constant ′ was dramatically increased as the proportion of CMCM/PSSF composites increased on the basis of Yoon-Nelson model, which suggested that structured fixed bed padded with CMSM/PSSF composite offered higher adsorption rate and mass transfer efficiency.

关键词： carbon molecular sieve membrane     stainless steel fibers     pyrolysis     structured fixed bed     toluene    

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Fabrication of a superhydrophilic/underwater superoleophobic stainless steel mesh for oil/water separation

《化学科学与工程前沿（英文）》 2023年 第17卷 第1期   页码 46-55 doi: 10.1007/s11705-022-2170-2

摘要： Because of the increasing amount of oily wastewater produced each day, it is important to develop superhydrophilic/underwater superoleophobic oil/water separation membranes with ultrahigh flux and high separation efficiency. In this paper, a superhydrophilic/underwater superoleophobic N-isopropylacrylamide-coated stainless steel mesh was prepared through a simple and convenient graft polymerization approach. The obtained mesh was able to separate oil/water mixtures only by gravity. In addition, the mesh showed high-efficiency separation ability (99.2%) and ultrahigh flux (235239 L∙m–2∙h–1). Importantly, due to the complex cross-linked bilayer structure, the prepared mesh exhibited good recycling performance and chemical stability in highly saline, alkaline and acidic environments.

关键词： oil/water separation     N-isopropylacrylamide     stainless steel mesh     ultrahigh flux    

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Evolution of composite fouling on a vertical stainless steel surface caused by treated sewage

Cheng ZAN, Lin SHI, Xiujuan MA, Wenyan YANG,

《能源前沿（英文）》 2010年 第4卷 第2期   页码 171-180 doi: 10.1007/s11708-009-0068-z

摘要： Composite biological and inorganic fouling occurs in plate heat exchangers (PHEs) using treated sewage as heat transfer medium, which lowers the heat transfer coefficient and increases the frictional resistance. In order to optimize the heat exchange process and improve the anti-fouling strategies, the dynamic behavior of composite fouling at a vertical surface of stainless steel (ANSI 316L) was investigated under typical conditions of PHEs. The growth curves of composite fouling were obtained. The evolution of composite fouling was characterized by means of environmental scanning electron microscopy (ESEM). Backscattered Electron Image (BEI) and energy dispersive X-ray spectrometry (EDS) were used as aids in interpreting the results. The experimental results show that a preliminary stage of a 6-day period with a low fouling growth rate exists during the composite fouling development. A significant change of the fouling growth rate happens after the preliminary stage during which the bacterial behaviors at the surface could be recorded clearly. After the preliminary stage, a space net-shape, mainly consisting of bacteria, extracellular products (EPS) and inorganic particles, could be established on the surface of the fouling layer. The change of fouling growth rate occurs synchronously with the evolution.

关键词： treated sewage     plate heat exchanger     stainless steel     composite fouling     biofouling    

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Orientation effect of electropolishing characteristics of 316L stainless steel fabricated by laser powder

《机械工程前沿（英文）》 2021年 第16卷 第3期   页码 580-592 doi: 10.1007/s11465-021-0633-7

摘要： 3D metal printing process has attracted increasing attention in recent years due to advantages, such as flexibility and rapid prototyping. This study aims to investigate the orientation effect of electropolishing characteristics on different surfaces of 316L stainless steel fabricated by laser powder bed fusion (L-PBF), considering that the rough surface of 3D printed parts is a key factor limiting its applications in the industry. The electropolishing characteristics on the different surfaces corresponding to the building orientation in selective laser melting are studied. Experimental results show that electrolyte temperature has critical importance on the electropolishing, especially for the vertical direction to the layering plane. The finish of electropolished surfaces is affected by the defects generated during L-PBF process. Thus, the electropolished vertical surface has higher surface roughness Sa than the horizontal surface. The X-ray photoelectron spectroscopy spectra show that the electropolished horizontal surface has higher Cr/Fe element ratio than the vertical surface. The electropolished horizontal surface presents higher corrosion resistance than the vertical surface by measuring the anodic polarization curves and fitting the equivalent circuit of experimental electrochemical impedance spectroscopy.

关键词： electropolishing     laser powder bed fusion     316L stainless steel     corrosion resistance     microstructure    

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On corrosion to stainless steel by calcium chloride with different extender

Lv XU, Yuanyang HU, Liwei WANG, Ruzhu WANG,

《能源前沿（英文）》 2010年 第4卷 第2期   页码 181-184 doi: 10.1007/s11708-009-0065-2

摘要： A calcium chloride solution with a different extender, which is made up of either pure calcium chloride, calcium chloride with expanded graphite, or calcium chloride with activated carbon, acts differently on stainless steel. The mass ratio between calcium chloride with expanded graphite or activated carbon is almost 4∶1, which is demonstrated to be the optimum ratio. The experimental research in this paper reveals that, of the three solutions, which are pure calcium chloride, calcium chloride with expanded graphite, and calcium chloride with activated carbon, the strongest oxidation creation and pitting corrosion happened in the solution of calcium chloride with expanded graphite, the weakest oxidation creation happened in the solution of calcium chloride with activated carbon, and pitting corrosion was stronger than oxidation creation in the solution of pure calcium chloride. This paper gives the reasons for these phenomena. Furthermore, based on theory analysis, multiple means and approaches are provided to prevent stainless steel from further corroding.

关键词： stainless steel     corrosion     calcium chloride     expanded graphite     activated carbon     oxidation creation     pitting corrosion    

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Axial compression behavior of CFRP-confined rectangular concrete-filled stainless steel tube stub column

《结构与土木工程前沿（英文）》 2021年 第15卷 第5期   页码 1144-1159 doi: 10.1007/s11709-021-0762-4

摘要： The mechanical properties of CFRP-confined rectangular concrete-filled stainless steel tube (CFSST) stub columns under axial compression were experimentally studied. A total of 28 specimens (7 groups) were fabricated for the axial compression test to study the influences of length-to-width ratio, CFRP constraint coefficient, and the thickness of stainless steel tube on the axial compression behavior. The specimen failure modes, the stress development of stainless steel tube and CFRP wrap, and the load–strain ratio curves in the loading process were obtained. Meanwhile, the relationship between axial and transverse deformations of each specimen was analyzed through the typical relative load−strain ratio curves. A bearing capacity prediction method was proposed based on the twin-shear strength theory, combining the limit equilibrium state of the CFRP-confined CFSST stub column under axial compression. The prediction method was calibrated by the test data in this study and other literature. The results show that the prediction method is of high accuracy.

关键词： CFRP     rectangular CFSST stub column     bearing capacity     limit equilibrium state     twin-shear strength theory    

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Characterization of landfilled stainless steel slags in view of metal recovery

Xuan Wang, Daneel Geysen, Tom Van Gerven, Peter T. Jones, Bart Blanpain, Muxing Guo

《化学科学与工程前沿（英文）》 2017年 第11卷 第3期   页码 353-362 doi: 10.1007/s11705-017-1656-9

摘要： The slag samples taken from landfill, which originated from different metallurgical processes, have been characterized in this study. The slags were categorized as electric arc furnace (EAF) slag, argon oxygen decarburization/metal refining process slag and vacuum oxygen decarburization slag based on chromium content and basicity. EAF slags have higher potential in metal recovery than the other two slags due to its higher iron and chromium contents. The size of the iron-chromium-nickel alloy particles varies from a few µm up to several cm. The recoveries of large metal particles and metal-spinel aggregates have potential to make the metal recovery from landfilled slags economically viable.

关键词： landfilled stainless steel slag     metal recovery     characterization    

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Fatigue crack growth behavior of a 170 mm diameter stainless steel straight pipe subjected to combined

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 905-913 doi: 10.1007/s11709-021-0683-2

摘要： In a nuclear powerplant, the rotary equipment, such as a pump directly fitted with hanger in the piping system, experiences torsional and bending loads. Higher crack growth rate occurs because of this torsional load in addition to the bending load. Hence, it is necessary to study the fatigue behavior of piping components under the influence of combined torsional and bending load. In this study, experimental fatigue life evaluation was conducted on a notched stainless steel SA312 Type 304LN straight pipe having an outer diameter of 170 mm. The experimental crack depth was measured using alternating current potential drop technique. The fatigue life of the stainless steel straight pipe was predicted using experiments, Delale and Erdogan method, and area-averaged root mean square–stress intensity factor approach at the deepest and surface points of the notch. Afterward, the fatigue crack growth and crack pattern were discussed. As a result, fatigue crack growth predicted using analytical methods are in good agreement with experimental results.

关键词： fatigue life     Delale and Erdogan method     RMS–SIF approach     stainless steel     torsion and bending load     fatigue crack growth    

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Numerical study of the cyclic load behavior of AISI 316L stainless steel shear links for seismic fuse

Ruipeng LI,Yunfeng ZHANG,Le-Wei TONG

《结构与土木工程前沿（英文）》 2014年 第8卷 第4期   页码 414-426 doi: 10.1007/s11709-014-0276-4

摘要： This paper presents the results of nonlinear finite element analyses conducted on stainless steel shear links. Stainless steels are attractive materials for seismic fuse device especially for corrosion-aware environment such as coastal regions because they are highly corrosion resistant, have good ductility and toughness properties in combination with low maintenance requirements. This paper discusses the promising use of AISI 316L stainless steel for shear links as seismic fuse devices. Hysteresis behaviors of four stainless steel shear link specimens under reversed cyclic loading were examined to assess their ultimate strength, plastic rotation and failure modes. The nonlinear finite element analysis results show that shear links made of AISI 316L stainless steel exhibit a high level of ductility. However, it is also found that because of large over-strength ratio associated with its strain hardening process, mixed shear and flexural failure modes were observed in stainless steel shear links compared with conventional steel shear links with the same length ratio. This raises the issue that proper design requirements such as length ratio, element compactness and stiffener spacing need to be determined to ensure the full development of the overall plastic rotation of the stainless steel shear links.

关键词： hysteretic damper     eccentrically braced frame     energy dissipation     seismic     stainless steel     shear link    

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Influence of the field humiture environment on the mechanical properties of 316L stainless steel repaired

Lianzhong ZHANG, Dichen LI, Shenping YAN, Ruidong XIE, Hongliang QU

《机械工程前沿（英文）》 2018年 第13卷 第4期   页码 513-519 doi: 10.1007/s11465-018-0503-0

摘要：

The mechanical properties of 316L stainless steel repaired with Fe314 under different temperatures and humidities without inert gas protection were studied. Results indicated favorable compatibility between Fe314 and 316L stainless steel. The average yield strength, tensile strength, and sectional contraction percentage were higher in repaired samples than in 316L stainless steel, whereas the elongation rate was slightly lower. The different conditions of humiture environment on the repair sample exerted minimal influence on tensile and yield strengths. The Fe314 cladding layer was mainly composed of equiaxed grains and mixed with randomly oriented columnar crystal and tiny pores or impurities in the tissue. Results indicated that the hardness value of Fe314 cladding layer under different humiture environments ranged within 419–451.1 HV0.2. The field humiture environment also showed minimal impact on the average hardness of Fe314 cladding layers. Furthermore, 316L stainless steel can be repaired through laser cladding by using Fe314 powder without inert gas protection under different temperatures and humidity environments.

关键词： laser cladding     repaired performance     tensile strength     temperature and humidity environment    

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Effect of fiber hybridization on energy absorption and synergy in concrete

Ahmadreza RAMEZANI, Mohammad Reza ESFAHANI

《结构与土木工程前沿（英文）》 2019年 第13卷 第6期   页码 1338-1349 doi: 10.1007/s17009-019-0558-2

摘要： In the present study, steel and polypropylene (PP) fibers have been utilized with the intent of obtaining hybrid fiber-reinforced concrete (HFRC) with desirable mechanical properties. An attempt has been made to scrutinize the properties of HFRC with the main concentration being on energy absorption characteristics of concrete and the efficacy of fiber hybridization in producing synergy. Accordingly, a total of 180 specimens, representing 20 different mixtures have been cast and evaluated through compressive, split tensile, and flexural tests. The relevant flexural toughness of the specimens was calculated using ASTM C1018, ASTM C1609, JSCE, and PCS methods, and the effectiveness of these methods was evaluated based on the experimental results. It was observed that steel fibers are more effective in the improvement of flexural toughness in the presence of PP fibers. Furthermore, synergy associated with the combination of fibers at different stages of deflection of the beam specimens was observed and analyzed.

关键词： hybrid fiber-reinforced concrete     synergy     toughness     steel fibers     polypropylene fibers    

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Preparation and permeability of ZSM-35 zeolite membranes on porous stainless steel tubes

ZHU Gang, WANG Jinqu, ZHANG Yan, LU Jinming, XIU Jinghai

《化学科学与工程前沿（英文）》 2007年 第1卷 第3期   页码 217-220 doi: 10.1007/s11705-007-0039-z

摘要： ZSM-35 zeolite membranes were prepared on porous stainless steel tubes with silica sol and tetraethoxysilane as silica source, and with 1-butylamine and ethylenediamine as templates, respectively. The characterization of X-ray diffraction (XRD) and scanning electron microscopy (SEM) showed that the membranes prepared with ethylenediamine as the template displayed growth orientation with their crystal planes (h00) parallel to the support surface. The single-component permeability tests of H, N and CH showed that the membranes synthesized with ethylenediamine as the template, compared with those with 1-butylamine as the template, showed relatively higher permeation rates and ideal separation factors, and above their corresponding ideal Knudsen diffusion factors, which might be attributed to the different growth orientation of zeolite membranes synthesized with different templates.

关键词： single-component permeability     diffusion     different     permeation     orientation    

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Process improvement in laser hot wire cladding for martensitic stainless steel based on the Taguchi method

Zilin HUANG,Gang WANG,Shaopeng WEI,Changhong LI,Yiming RONG

《机械工程前沿（英文）》 2016年 第11卷 第3期   页码 242-249 doi: 10.1007/s11465-016-0397-7

摘要：

Laser hot wire cladding, with the prominent features of low heat input, high energy efficiency, and high precision, is widely used for remanufacturing metal parts. The cladding process, however, needs to be improved by using a quantitative method. In this work, volumetric defect ratio was proposed as the criterion to describe the integrity of forming quality for cladding layers. Laser deposition experiments with FV520B, one of martensitic stainless steels, were designed by using the Taguchi method. Four process variables, namely, laser power (P), scanning speed (Vs), wire feed rate (Vf), and wire current (I), were optimized based on the analysis of signal-to-noise (S/N) ratio. Metallurgic observation of cladding layer was conducted to compare the forming quality and to validate the analysis method. A stable and continuous process with the optimum parameter combination produced uniform microstructure with minimal defects and cracks, which resulted in a good metallurgical bonding interface.

关键词： process optimization     Taguchi method     signal-to-noise (S/N) ratio     volumetric defect ratio     laser hot wire cladding    

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Experimental study on mechanical properties of a novel micro-steel fiber reinforced magnesium phosphate

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 1047-1057 doi: 10.1007/s11709-021-0755-3

摘要： Magnesium phosphate cement (MPC) received increased attention in recent years, but MPC-based concrete is rarely reported. The micro-steel fibers (MSF) were added to MPC-based concrete to enhance its ductility due to the high brittleness in tensile and flexural strength properties of MPC. This paper investigates the effect of MSF volume fraction on the mechanical properties of a new pattern of MPC-based concrete. The temperature development curve, fluidity, cubic compressive strength, modulus of elastic, axial compressive strength, and four-point flexural strength were experimentally studied with 192 specimens, and a scanning electron microscopy (SEM) test was carried out after the specimens were failed. Based on the test results, the correlations between the cubic compressive strength and curing age, the axial and cubic compressive strength of MPC-based concrete were proposed. The results showed that with the increase of MSF volume fraction, the fluidity of fresh MPC-based concrete decreased gradually. MSF had no apparent influence on the compressive strength, while it enhanced the four-point flexural strength of MPC-based concrete. The four-point flexural strength of specimens with MSF volume fraction from 0.25% to 0.75% were 12.3%, 21.1%, 24.6% higher than that of the specimens without MSF, respectively.

关键词： magnesium phosphate cement-based concrete     micro-steel fibers     four-point flexural strength     compressive strength    

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高性能节约型不锈钢制备技术研发与应用

谢胜涛,刘振宇,王国栋

《中国工程科学》 2014年 第16卷 第1期   页码 81-87

摘要：

开发了409L和410S铁素体不锈钢冷轧板的淬火-配分（Q&P）工艺，获得了铁素体、马氏体和残余奥氏体的复相组织。通过优化奥氏化温度、淬火温度和配分时间，获得了尽量多的马氏体和残余奥氏体。与常规退火和淬火-回火（Q&T）工艺相比，Q&P工艺获得了最优的强度和延伸率组合、连续性屈服和适中的n值、r值，达到了高强度和易成型的要求，能够替代先进高强钢用于生产汽车结构件。

关键词： 不锈钢     淬火     配分     高强度     易成型    

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标题 作者 时间 类型 操作

Preparation and characterization of novel carbon molecular sieve membrane/PSSF composite by pyrolysis method for toluene adsorption

Ying Yan, Peng Huang, Huiping Zhang

期刊论文

Fabrication of a superhydrophilic/underwater superoleophobic stainless steel mesh for oil/water separation

期刊论文

Evolution of composite fouling on a vertical stainless steel surface caused by treated sewage

Cheng ZAN, Lin SHI, Xiujuan MA, Wenyan YANG,

期刊论文

Orientation effect of electropolishing characteristics of 316L stainless steel fabricated by laser powder

期刊论文

On corrosion to stainless steel by calcium chloride with different extender

Lv XU, Yuanyang HU, Liwei WANG, Ruzhu WANG,

期刊论文

Axial compression behavior of CFRP-confined rectangular concrete-filled stainless steel tube stub column

期刊论文

Characterization of landfilled stainless steel slags in view of metal recovery

Xuan Wang, Daneel Geysen, Tom Van Gerven, Peter T. Jones, Bart Blanpain, Muxing Guo

期刊论文

Fatigue crack growth behavior of a 170 mm diameter stainless steel straight pipe subjected to combined

期刊论文

Numerical study of the cyclic load behavior of AISI 316L stainless steel shear links for seismic fuse

Ruipeng LI,Yunfeng ZHANG,Le-Wei TONG

期刊论文

Influence of the field humiture environment on the mechanical properties of 316L stainless steel repaired

Lianzhong ZHANG, Dichen LI, Shenping YAN, Ruidong XIE, Hongliang QU

期刊论文

Effect of fiber hybridization on energy absorption and synergy in concrete

Ahmadreza RAMEZANI, Mohammad Reza ESFAHANI

期刊论文

Preparation and permeability of ZSM-35 zeolite membranes on porous stainless steel tubes

ZHU Gang, WANG Jinqu, ZHANG Yan, LU Jinming, XIU Jinghai

期刊论文

Process improvement in laser hot wire cladding for martensitic stainless steel based on the Taguchi method

Zilin HUANG,Gang WANG,Shaopeng WEI,Changhong LI,Yiming RONG

期刊论文

Experimental study on mechanical properties of a novel micro-steel fiber reinforced magnesium phosphate

期刊论文

高性能节约型不锈钢制备技术研发与应用

谢胜涛,刘振宇,王国栋

期刊论文